NickelMaghrebV1, France, Analysis, bibRecord, 000084

Electrochemical Boron-Doped Diamond Film Microcells Micromachined with Femtosecond Laser: Application to the Determination of Water Framework Directive Metals

Identifieur interne : 000084 ( France/Analysis ); précédent : 000083; suivant : 000085

Electrochemical Boron-Doped Diamond Film Microcells Micromachined with Femtosecond Laser: Application to the Determination of Water Framework Directive Metals

Auteurs : Amel Sbartai [France, Algérie] ; Philippe Namour [France] ; Abdelhamid Errachid [France] ; Jan Krejci [République tchèque] ; Romana Sejnohova [République tchèque] ; Louis Renaud [France] ; Mohamed Larbi Hamlaoui [Algérie] ; Anne-Sophie Loir [Belgique] ; Florence Garrelie [Belgique] ; Christophe Donnet [Belgique] ; Herve Soder [Belgique] ; Eric Audouard [Belgique] ; Julien Granier [Belgique] ; Nicole Jaffrezic-Renault [France]

Source :

Analytical chemistry : (Washington) [ 0003-2700 ] ; 2012.

RBID : Pascal:12-0358527

Descripteurs français

Pascal (Inist)
- Méthode électrochimique, Bore, Laser, Application, Evaluation performance, Voltampérométrie impulsion différentielle, Voltammétrie redissolution anodique, Ion métallique, Limite détection, Linéarité, Environnement, Qualité, Etalon, Concentration, Diamant, Eau, Métal lourd, Cadmium II, Nickel II, Plomb II, Mercure II.
Wicri :
- topic : Eau, Métal lourd.

English descriptors

KwdEn :
- Anodic stripping voltammetry, Application, Boron, Cadmium II, Concentration, Detection limit, Diamond, Differential impulse voltamperometry, Electrochemical method, Environment, Heavy metal, Laser, Lead II, Linearity, Mercury II, Metal ion, Nickel II, Performance evaluation, Quality, Standard, Water.

Abstract

Planar electrochemical microcells were micromachined in a microcrystalline boron-doped diamond (BDD) thin layer using a femtosecond laser. The electrochemical performances of the new laser-machined BDD microcell were assessed by differential pulse anodic stripping voltammetry (DPASV) determinations, at the nanomolar level, of the four heavy metal ions of the European Water Framework Directive (WFD): Cd(II), Ni(II), Pb(II), Hg(II). The results are compared with those of previously published BDD electrodes. The calculated detection limits are 0.4, 6.8, 5.5, and 2.3 nM, and the linearities go up to 35, 97, 48, and 5 nM for, respectively, Cd(II), Ni(II) Pb(II), and Hg(II). The detection limits meet with the environmental quality standard of the WFD for three of the four metals. It was shown that the four heavy metals could be detected simultaneously in the concentration ratio usually measured in sewage or runoff waters.

Affiliations:

Links toward previous steps (curation, corpus...)

to stream PascalFrancis, to step Corpus: 000081
to stream PascalFrancis, to step Curation: 000360
to stream PascalFrancis, to step Checkpoint: 000093
to stream Main, to step Merge: 000290
to stream Main, to step Curation: 000284
to stream Main, to step Exploration: 000284
to stream France, to step Extraction: 000084

Links to Exploration step

Pascal:12-0358527

Le document en format XML

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<sourceDesc><biblStruct><analytic><title xml:lang="en" level="a">Electrochemical Boron-Doped Diamond Film Microcells Micromachined with Femtosecond Laser: Application to the Determination of Water Framework Directive Metals</title>
<author><name sortKey="Sbartai, Amel" sort="Sbartai, Amel" uniqKey="Sbartai A" first="Amel" last="Sbartai">Amel Sbartai</name>
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<s2>69622, Villeurbanne</s2>
<s3>FRA</s3>
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<s3>FRA</s3>
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<author><name sortKey="Hamlaoui, Mohamed Larbi" sort="Hamlaoui, Mohamed Larbi" uniqKey="Hamlaoui M" first="Mohamed Larbi" last="Hamlaoui">Mohamed Larbi Hamlaoui</name>
<affiliation wicri:level="1"><inist:fA14 i1="04"><s1>University of Annaba, Laboratoire EPEV, BP 12, El Hadjar</s1>
<s2>23000 Annaba</s2>
<s3>DZA</s3>
<sZ>1 aut.</sZ>
<sZ>7 aut.</sZ>
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<country>Algérie</country>
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<author><name sortKey="Loir, Anne Sophie" sort="Loir, Anne Sophie" uniqKey="Loir A" first="Anne-Sophie" last="Loir">Anne-Sophie Loir</name>
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<s2>Saint-Etienne</s2>
<s3>BEL</s3>
<sZ>8 aut.</sZ>
<sZ>9 aut.</sZ>
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<country>Belgique</country>
<placeName><settlement type="city">Saint-Étienne</settlement>
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</author>
<author><name sortKey="Garrelie, Florence" sort="Garrelie, Florence" uniqKey="Garrelie F" first="Florence" last="Garrelie">Florence Garrelie</name>
<affiliation wicri:level="4"><inist:fA14 i1="05"><s1>University of Lyon, Laboratoire Hubert Curien, UMR CNRS 5516, Université Jean Monnet Saint-Etienne</s1>
<s2>Saint-Etienne</s2>
<s3>BEL</s3>
<sZ>8 aut.</sZ>
<sZ>9 aut.</sZ>
<sZ>10 aut.</sZ>
</inist:fA14>
<country>Belgique</country>
<placeName><settlement type="city">Saint-Étienne</settlement>
<region type="region" nuts="2">Auvergne-Rhône-Alpes</region>
<region type="old region" nuts="2">Rhône-Alpes</region>
</placeName>
<orgName type="university">Université Jean Monnet Saint-Etienne</orgName>
<orgName type="institution" wicri:auto="newGroup">Université de Lyon</orgName>
</affiliation>
</author>
<author><name sortKey="Donnet, Christophe" sort="Donnet, Christophe" uniqKey="Donnet C" first="Christophe" last="Donnet">Christophe Donnet</name>
<affiliation wicri:level="4"><inist:fA14 i1="05"><s1>University of Lyon, Laboratoire Hubert Curien, UMR CNRS 5516, Université Jean Monnet Saint-Etienne</s1>
<s2>Saint-Etienne</s2>
<s3>BEL</s3>
<sZ>8 aut.</sZ>
<sZ>9 aut.</sZ>
<sZ>10 aut.</sZ>
</inist:fA14>
<country>Belgique</country>
<placeName><settlement type="city">Saint-Étienne</settlement>
<region type="region" nuts="2">Auvergne-Rhône-Alpes</region>
<region type="old region" nuts="2">Rhône-Alpes</region>
</placeName>
<orgName type="university">Université Jean Monnet Saint-Etienne</orgName>
<orgName type="institution" wicri:auto="newGroup">Université de Lyon</orgName>
</affiliation>
</author>
<author><name sortKey="Soder, Herve" sort="Soder, Herve" uniqKey="Soder H" first="Herve" last="Soder">Herve Soder</name>
<affiliation wicri:level="1"><inist:fA14 i1="06"><s1>Société IMPULSION SAS, 12, Rue Barrouin</s1>
<s2>42000 Saint-Etienne</s2>
<s3>BEL</s3>
<sZ>11 aut.</sZ>
<sZ>12 aut.</sZ>
<sZ>13 aut.</sZ>
</inist:fA14>
<country>Belgique</country>
<wicri:noRegion>42000 Saint-Etienne</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Audouard, Eric" sort="Audouard, Eric" uniqKey="Audouard E" first="Eric" last="Audouard">Eric Audouard</name>
<affiliation wicri:level="1"><inist:fA14 i1="06"><s1>Société IMPULSION SAS, 12, Rue Barrouin</s1>
<s2>42000 Saint-Etienne</s2>
<s3>BEL</s3>
<sZ>11 aut.</sZ>
<sZ>12 aut.</sZ>
<sZ>13 aut.</sZ>
</inist:fA14>
<country>Belgique</country>
<wicri:noRegion>42000 Saint-Etienne</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Granier, Julien" sort="Granier, Julien" uniqKey="Granier J" first="Julien" last="Granier">Julien Granier</name>
<affiliation wicri:level="1"><inist:fA14 i1="06"><s1>Société IMPULSION SAS, 12, Rue Barrouin</s1>
<s2>42000 Saint-Etienne</s2>
<s3>BEL</s3>
<sZ>11 aut.</sZ>
<sZ>12 aut.</sZ>
<sZ>13 aut.</sZ>
</inist:fA14>
<country>Belgique</country>
<wicri:noRegion>42000 Saint-Etienne</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Jaffrezic Renault, Nicole" sort="Jaffrezic Renault, Nicole" uniqKey="Jaffrezic Renault N" first="Nicole" last="Jaffrezic-Renault">Nicole Jaffrezic-Renault</name>
<affiliation wicri:level="3"><inist:fA14 i1="01"><s1>University of Lyon, Institute of Analytical Sciences, UMR CNRS 5280, Universite Claude Bernard Lyon 1, 43 Boulevard 11 Nnovembre 1918</s1>
<s2>69622, Villeurbanne</s2>
<s3>FRA</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>14 aut.</sZ>
</inist:fA14>
<country>France</country>
<placeName><region type="region" nuts="2">Auvergne-Rhône-Alpes</region>
<region type="old region" nuts="2">Rhône-Alpes</region>
<settlement type="city">Villeurbanne</settlement>
<settlement type="city" wicri:auto="agglo">Lyon</settlement>
</placeName>
</affiliation>
</author>
</analytic>
<series><title level="j" type="main">Analytical chemistry : (Washington)</title>
<title level="j" type="abbreviated">Anal. chem. : (Wash. DC)</title>
<idno type="ISSN">0003-2700</idno>
<imprint><date when="2012">2012</date>
</imprint>
</series>
</biblStruct>
</sourceDesc>
<seriesStmt><title level="j" type="main">Analytical chemistry : (Washington)</title>
<title level="j" type="abbreviated">Anal. chem. : (Wash. DC)</title>
<idno type="ISSN">0003-2700</idno>
</seriesStmt>
</fileDesc>
<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Anodic stripping voltammetry</term>
<term>Application</term>
<term>Boron</term>
<term>Cadmium II</term>
<term>Concentration</term>
<term>Detection limit</term>
<term>Diamond</term>
<term>Differential impulse voltamperometry</term>
<term>Electrochemical method</term>
<term>Environment</term>
<term>Heavy metal</term>
<term>Laser</term>
<term>Lead II</term>
<term>Linearity</term>
<term>Mercury II</term>
<term>Metal ion</term>
<term>Nickel II</term>
<term>Performance evaluation</term>
<term>Quality</term>
<term>Standard</term>
<term>Water</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Méthode électrochimique</term>
<term>Bore</term>
<term>Laser</term>
<term>Application</term>
<term>Evaluation performance</term>
<term>Voltampérométrie impulsion différentielle</term>
<term>Voltammétrie redissolution anodique</term>
<term>Ion métallique</term>
<term>Limite détection</term>
<term>Linéarité</term>
<term>Environnement</term>
<term>Qualité</term>
<term>Etalon</term>
<term>Concentration</term>
<term>Diamant</term>
<term>Eau</term>
<term>Métal lourd</term>
<term>Cadmium II</term>
<term>Nickel II</term>
<term>Plomb II</term>
<term>Mercure II</term>
</keywords>
<keywords scheme="Wicri" type="topic" xml:lang="fr"><term>Eau</term>
<term>Métal lourd</term>
</keywords>
</textClass>
</profileDesc>
</teiHeader>
<front><div type="abstract" xml:lang="en">Planar electrochemical microcells were micromachined in a microcrystalline boron-doped diamond (BDD) thin layer using a femtosecond laser. The electrochemical performances of the new laser-machined BDD microcell were assessed by differential pulse anodic stripping voltammetry (DPASV) determinations, at the nanomolar level, of the four heavy metal ions of the European Water Framework Directive (WFD): Cd(II), Ni(II), Pb(II), Hg(II). The results are compared with those of previously published BDD electrodes. The calculated detection limits are 0.4, 6.8, 5.5, and 2.3 nM, and the linearities go up to 35, 97, 48, and 5 nM for, respectively, Cd(II), Ni(II) Pb(II), and Hg(II). The detection limits meet with the environmental quality standard of the WFD for three of the four metals. It was shown that the four heavy metals could be detected simultaneously in the concentration ratio usually measured in sewage or runoff waters.</div>
</front>
</TEI>
<affiliations><list><country><li>Algérie</li>
<li>Belgique</li>
<li>France</li>
<li>République tchèque</li>
</country>
<region><li>Auvergne-Rhône-Alpes</li>
<li>Rhône-Alpes</li>
</region>
<settlement><li>Lyon</li>
<li>Saint-Étienne</li>
<li>Villeurbanne</li>
</settlement>
<orgName><li>Université Jean Monnet Saint-Etienne</li>
<li>Université de Lyon</li>
</orgName>
</list>
<tree><country name="France"><region name="Auvergne-Rhône-Alpes"><name sortKey="Sbartai, Amel" sort="Sbartai, Amel" uniqKey="Sbartai A" first="Amel" last="Sbartai">Amel Sbartai</name>
</region>
<name sortKey="Errachid, Abdelhamid" sort="Errachid, Abdelhamid" uniqKey="Errachid A" first="Abdelhamid" last="Errachid">Abdelhamid Errachid</name>
<name sortKey="Jaffrezic Renault, Nicole" sort="Jaffrezic Renault, Nicole" uniqKey="Jaffrezic Renault N" first="Nicole" last="Jaffrezic-Renault">Nicole Jaffrezic-Renault</name>
<name sortKey="Namour, Philippe" sort="Namour, Philippe" uniqKey="Namour P" first="Philippe" last="Namour">Philippe Namour</name>
<name sortKey="Namour, Philippe" sort="Namour, Philippe" uniqKey="Namour P" first="Philippe" last="Namour">Philippe Namour</name>
<name sortKey="Renaud, Louis" sort="Renaud, Louis" uniqKey="Renaud L" first="Louis" last="Renaud">Louis Renaud</name>
</country>
<country name="Algérie"><noRegion><name sortKey="Sbartai, Amel" sort="Sbartai, Amel" uniqKey="Sbartai A" first="Amel" last="Sbartai">Amel Sbartai</name>
</noRegion>
<name sortKey="Hamlaoui, Mohamed Larbi" sort="Hamlaoui, Mohamed Larbi" uniqKey="Hamlaoui M" first="Mohamed Larbi" last="Hamlaoui">Mohamed Larbi Hamlaoui</name>
</country>
<country name="République tchèque"><noRegion><name sortKey="Krejci, Jan" sort="Krejci, Jan" uniqKey="Krejci J" first="Jan" last="Krejci">Jan Krejci</name>
</noRegion>
<name sortKey="Sejnohova, Romana" sort="Sejnohova, Romana" uniqKey="Sejnohova R" first="Romana" last="Sejnohova">Romana Sejnohova</name>
</country>
<country name="Belgique"><region name="Auvergne-Rhône-Alpes"><name sortKey="Loir, Anne Sophie" sort="Loir, Anne Sophie" uniqKey="Loir A" first="Anne-Sophie" last="Loir">Anne-Sophie Loir</name>
</region>
<name sortKey="Audouard, Eric" sort="Audouard, Eric" uniqKey="Audouard E" first="Eric" last="Audouard">Eric Audouard</name>
<name sortKey="Donnet, Christophe" sort="Donnet, Christophe" uniqKey="Donnet C" first="Christophe" last="Donnet">Christophe Donnet</name>
<name sortKey="Garrelie, Florence" sort="Garrelie, Florence" uniqKey="Garrelie F" first="Florence" last="Garrelie">Florence Garrelie</name>
<name sortKey="Granier, Julien" sort="Granier, Julien" uniqKey="Granier J" first="Julien" last="Granier">Julien Granier</name>
<name sortKey="Soder, Herve" sort="Soder, Herve" uniqKey="Soder H" first="Herve" last="Soder">Herve Soder</name>
</country>
</tree>
</affiliations>
</record>

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Electrochemical Boron-Doped Diamond Film Microcells Micromachined with Femtosecond Laser: Application to the Determination of Water Framework Directive Metals

Electrochemical Boron-Doped Diamond Film Microcells Micromachined with Femtosecond Laser: Application to the Determination of Water Framework Directive Metals

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